MEL-BUILD Double tilt LN2 Atmos Defend Holder

vacuum transfer

High stability is essential for acquiring atomic-scale information by transmission electron microscopy (TEM). This is especially true in the case with materials that are susceptible to beam damage that require cooling to Cryogenic temperatures. The MEL-BUILD Double tilt LN2 Atmos Defend Holder is designed specifically for the material scientist. Ideal for Lithium-Ion Battery research this newly designed Double Tilt LN2 TEM holder incorporates a specially designed vacuum transfer system and a proprietary mechanical drift cancellation controller. This combined with a high precision temperature controller which range is ± 0.005°C allows for stable and repeatable acquisition of data.  In addition, the double tilt mechanism allows the TEM microscopist to match the crystal orientation, making it the only LN2 TEM holder in the world that allows atomic resolution observation.

vacuum transfer
Component Double-tilt, LN2 Cooling and Vacuum Transfer
Ultimate temp -160°C
Reaching time : 60min
X tilt : ±25°
Y tilt / Min step : ±20°/ 0.05°
Sample set : Smart Set System
Coolant LN2 : replenish LN2 repeatedly
TEM : JEOL PP type HR/FHP/UHR
Thermofisher
TFS Include item:
Temp. controller, Y tilt controller,
Software, Safety Operation Stand of TEM holder introduce.
close up

HR-TEM observation Au nano particles on cross grating was performed immediately after temperature reached in -170 ℃ (cooling time 60 min). Image collected on the JEOL ARM 200F TEM.

vacuum transfer close up

EDS mapping of SrTiO3 using the MEL-BUILD LN2 cooling holder. Images care of Dr. Kumamoto, Dr. Nakayama, Dr. Ishikawa and Prof. Shibata Prof. Ikuhara of the University of Tokyo.

close up 2

The above image is an Atomic resolution STEM image of LLZ(Li7La3Zr2O12), From this result, it was proven that the non-exposure (Vacuum Transfer) was successful. The crystal orientation was adjusted by Y tilt, and the electron beam damage was reduced by cooling of -160°C. Cooling and stability was achieved in 60 minutes.